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More about chromatography

Rtx-35 MS

(Crossbond® 35% diphenyl/65% dimethyl polysiloxane)GC column

  • Midpolarity phase.
  • Column specifically tested for low bleed performance.
  • Equivalent to USP G42 phase.
  • Rtx®-35 columns are available with Integra-Guard™ built-in guard column.

An Rtx®-35 column is a popular confirmation column for pesticides and herbicides, in conjunction with an Rtx®-5 or Rtx®-1701 column. The higher phenyl content causes useful elution order and retention time changes.

Applications
  • Organochlorine pesticides
  • PCB congeners or Aroclor mixes
  • Herbicides
  • Pharmaceuticals
  • Sterols
  • Rosin acids
  • Phtalate esters
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.25 0.10 40 to 320/340
0.25 0.25 40 to 320/340
0.25 0.50 40 to 310/330
0.25 1.00 40 to 290/310
0.32 0.10 40 to 320/340
0.32 0.25 40 to 320/340
0.32 0.50 40 to 310/330
0.32 1.00 40 to 290310
0.53 0.50 40 to 300/320
0.53 1.00 40 to 290
0.53 1.50 40 to 280/300

Rtx-50

(Crossbond® 100%methylphenyl polysiloxane)GC column

  • Midpolarity phase.
  • Equivalent to USP G3 phase.

The high thermal stability of Rtx®-50 columns makes possible dual-column analysis with common phases such as Rtx®-1ms or Rtx®-5ms. Between analyses, high temperatures can be used to drive less volatile contaminants off of the column.

Applications
  • Organochlorine pesticides
  • Herbicides
  • Rosin acids
  • Sterols
  • Triglycerides
  • Phtalate esters
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.18 0.20 40 to 310/330
0.18 0.40 40 to 300/320
0.25 0.25 40 to 300/320
0.25 0.50 40 to 290/310
0.25 1.00 40 to 280/300
0.32 0.25 40 to 300/320
0.32 0.50 40 to 290/310
0.32 1.00 40 to 280/300
0.53 0.25 40 to 280/300
0.53 0.50 40 to 270/290
0.53 0.83 40 to 270/290
0.53 1.00 40 to 260/280
0.53 1.50 40 to 250/270

Rtx-65

(Crossbond® 65% diphenyl/35%dimethyl polysiloxane)GC column

  • Mid to high polarity phase.
  • Equivalent to USP G17 phase.

The Rtx®-65 phase contains the highest phenyl content of any bonded stationary phase available, to improve separation of aromatic compounds through increased phase-analyte interaction. A unique polarity makes these columns ideal for a variety of analyses, from phenols to FAMEs. As a confirmation column for EPA Method 604 phenols, an Rtx®-65 column produces a different elution order, compared to the primary Rtx®-5 column. Rtx®-65 columns elute FAMEs according to equivalent chain length, similar to bonded Carbowax® columns, but the Rtx®-65 phase does not suffer the thermal stability limitations of other polar stationary phases.

Applications
  • Phenols
  • Fatty acids
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.25 0.25 50 to 300
0.25 0.50 50 to 280/300
0.25 1.00 50 to 260/280
0.32 0.25 50 to 300
0.32 0.50 50 to 280/300
0.32 1.00 50 to 300
0.53 0.25 40 to 290/300
0.53 0.50 40 to 270/290
0.53 1.00 40 to 250/270

Rtx-440

(Proprietary Crossbond® phase)GC column

  • Intermediate polarity phase.
  • Low bleed
  • High-resolution columns with unique selectivity.
  • Ideal for low/trace level analysis.
Applications
  • Pesticides
  • PAHs
  • Semivolatiles
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.18 0.18 20 to 320/340
0.25 0.25 20 to 320/340
0.25 0.50 20 to 320/340
0.32 0.25 20 to 320/340
0.32 0.50 20 to 320/340
0.53 0.50 20 to 320/340
0.53 1.00 20 to 320/340

Stx-500

(Crossbond® carborane/dimethyl polysiloxane)GC column

  • Stx™ is used for columns that have been deactivated using Restek´s Siltek® deactivation.
  • Low bleed - ideal for GC/FPD, GC/NPD or GC/MS analyses.
Applications
  • Brominated flame retardans
  • Coplanar PCB congeners
  • other anates with high boiling temperatures
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.25 0.15 -60 to 380°C
0.53 0.15 -60 to 380°C

Rxi-17

Rxi® Capillary GC ColumnsGC column

These columns have been designed specifically to be the best columns available, for exceptional inertness, ultra-low bleed, and reproducible retention and selectivity. In addition to outstanding performance, this combination of column characteristics assures Rxi® columns will have long lifetimes. The Restek chemists also have developed a stable, reproducible manufacturing process, so that Rxi® columns will meet your needs every time you install a new column.

Benefits of Rxi® columns
  • Ultra-low bleed
  • Exceptional inertness
  • Reproducible performance, column after column
Applications
  • Pesticides
  • Herbicides
  • Rosin acids
  • Phthalate esters
  • Triglycerides
  • Sterols
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.10 0.10 40 to 280/320
0.25 0.25 40 to 280/320
0.25 0.50 40 to 280/320
0.25 1.00 40 to 280/320
0.32 0.25 40 to 280/320
0.32 0.50 40 to 280/320
0.32 1.00 40 to 280/320
0.53 0.25 40 to 280/320
0.53 0.50 40 to 280/320
0.53 0.83 40 to 280/320
0.53 1.00 40 to 280/320
0.53 1.50 40 to 280/320

Rxi-XLB

(low-polarity proprietary phase)

Rxi® Capillary GC ColumnsGC column

These columns have been designed specifically to be the best columns available, for exceptional inertness, ultra-low bleed, and reproducible retention and selectivity. In addition to outstanding performance, this combination of column characteristics assures Rxi® columns will have long lifetimes. The Restek chemists also have developed a stable, reproducible manufacturing process, so that Rxi® columns will meet your needs every time you install a new column.

Benefits of Rxi®-XLB columns
  • Ultra-low bleed
  • Exceptional inertness
  • Unique selectivity
  • Reproducible performance, column after column

Improvements in polymer synthesis and tubing deactivation enable us to make inert, stable Rxi®-XLB columns especially well-suited for analyzing active, high molecular weight compounds with sensitive GC/MS systems, including ion trap detectors. Excellent efficiency, coupled with inertness, low bleed, and high thermal stability, make Rxi®-XLB columns ideal for analyzing semivolatile compounds in drinking water (e.g., US EPA Method 525).

Applications
  • Pesticides
  • PCB congeners or (e.g.) Aroclor mixes
  • PAHs
Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.10 0.10 30 to 340/360
0.18 0.18 30 to 340/360
0.20 0.33 30 to 340/360
0.25 0.10 30 to 340/360
0.25 0.25 30 to 340/360
0.25 0.50 30 to 340/360
0.25 1.00 30 to 340/360
0.32 0.10 30 to 340/360
0.32 0.25 30 to 340/360
0.32 0.50 30 to 340/360
0.32 1.00 30 to 340/360
0.53 0.50 30 to 320/340
0.53 1.50 30 to 320/340

Rxi-5sil MS

Rxi® Capillary GC ColumnsGC column

These columns have been designed specifically to be the best columns available, for exceptional inertness, ultra-low bleed, and reproducible retention and selectivity. In addition to outstanding performance, this combination of column characteristics assures Rxi® columns will have long lifetimes. The Restek chemists also have developed a stable, reproducible manufacturing process, so that Rxi® columns will meet your needs every time you install a new column.

Benefits of Rxi® columns
  • Ultra-low bleed
  • Exceptional inertness
  • Reproducible performance, column after column

The Rxi®-5Sil MS stationary phase incorporates phenyl groups in the polymer backbone. This improves thermal stability, reduces bleed, and makes the phase less prone to oxidation. Rxi®-5Sil MS columns are ideal for GC/MS applications requiring high sensitivity, including use in ion trap systems.

Applications
  • Chlorinated hydrocarbons
  • Phthalates
  • Phenols
  • Amines
  • Organochlorine pesticides
  • Organophosphorus pesticides
  • Drugs
  • Solvent impurities
  • Hydrocarbons

Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.10 0.10 -60 to 330/350
0.18 0.18 -60 to 330/350
0.18 0.36 -60 to 330/350
0.25 0.10 -60 to 330/350
0.25 0.25 -60 to 330/350
0.25 0.50 -60 to 330/350
0.25 1.00 -60 to 325/350
0.32 0.25 -60 to 330/350
0.32 0.50 -60 to 330/350
0.32 1.00 -60 to 330/350
0.53 0.25 -60 to 325/350
0.53 1.50 -60 to 310/330

Rxi-5 MS

GC columnRxi® Capillary GC Columns

These columns have been designed specifically to be the best columns available, for exceptional inertness, ultra-low bleed, and reproducible retention and selectivity. In addition to outstanding performance, this combination of column characteristics assures Rxi® columns will have long lifetimes. The Restek chemists also have developed a stable, reproducible manufacturing process, so that Rxi® columns will meet your needs every time you install a new column.

Benefits of Rxi® columns
  • Ultra-low bleed
  • Exceptional inertness
  • Reproducible performance, column after column
Applications
  • Semivolatiles
  • Phenols
  • Amines
  • Residual solvents
  • Drugs of abuse
  • Pesticides
  • PCB congeners or (e.g.) Aroclor mixes
  • Solvent impurities

Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.10 0.10 -60 to 330/350
0.18 0.18 -60 to 330/350
0.18 0.30 -60 to 330/350
0.18 0.36 -60 to 330/350
0.20 0.33 -60 to 330/350
0.25 0.25 -60 to 330/350
0.25 0.40 -60 to 330/350
0.25 0.50 -60 to 330/350
0.25 1.00 -60 to 330/350
0.32 0.25 -60 to 330/350
0.32 0.50 -60 to 330/350
0.32 1.00 -60 to 330/350
0.53 0.25 -60 to 330/350
0.53 0.50 -60 to 330/350
0.53 1.00 -60 to 330/350
0.53 1.50 -60 to 330/350

Rxi-1 MS

GC columnRxi® Capillary GC Columns

These columns have been designed specifically to be the best columns available, for exceptional inertness, ultra-low bleed, and reproducible retention and selectivity. In addition to outstanding performance, this combination of column characteristics assures Rxi® columns will have long lifetimes. The Restek chemists also have developed a stable, reproducible manufacturing process, so that Rxi® columns will meet your needs every time you install a new column.

Benefits of Rxi® columns
  • Ultra-low bleed
  • Exceptional inertness
  • Reproducible performance, column after column
Applications
  • Drugs of abuse
  • Essential oils
  • Hydrocarbons
  • Pesticides
  • PCB congeners and Aroclor mixtures
  • Sulphur compounds
  • Amines
  • Solvent impurities
  • Simulated distillation
  • Oxygenates
  • Gasoline
  • Refinery gases

Temperature limits
ID (mm) df(µm) Temperature limits (°C)
0.10 0.10 -60 to 330/350
0.18 0.18 -60 to 330/350
0.18 0.36 -60 to 330/350
0.20 0.33 -60 to 330/350
0.25 0.25 -60 to 330/350
0.25 0.50 -60 to 330/350
0.25 1.00 -60 to 330/350
0.32 0.25 -60 to 330/350
0.32 0.50 -60 to 330/350
0.32 1.00 -60 to 330/350
0.32 4.00 -60 to 330/350
0.53 0.50 -60 to 330/350
0.53 1.00 -60 to 330/350
0.53 1.50 -60 to 330/350